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ChemicalBook--->CAS DataBase List--->2749-59-9

2749-59-9

2749-59-9 Structure

2749-59-9 Structure
IdentificationMore
[Name]

1,3-Dimethyl-5-pyrazolone
[CAS]

2749-59-9
[Synonyms]

1,3-dimethyl-2-pyrazolin-5-one
1,3-DIMETHYL-4,5-DIHYDRO-1H-PYRAZOL-5-ONE
1,3-DIMETHYL-5-PYRAZOLONE
1,3-DIMETHYLPYRAZOLONE
2,4-DIHYDRO-2,5-DIMETHYL-3H-PYRAZOL-3-ONE
BUTTPARK 82\11-61
1,3-Dimethyl-5-pyrazolinone
2,5-Dimethyl-2,4-dihydro-3H-pyrazol-3-one
2-Pyrazolin-5-one, 1,3-dimethyl-
1,3-dimethyl-5-pyrazolone(DMP)
3H-PYRAZOL-3-ONE, 2,4-DIHYDRO-2,5-DIMETHYL-
1,3-dimethyl-1H-pyrazol-5(4H)-one
1,3-DIMETHYL-5-PYRAZOLONE 95+%
2,5-Dimethyl-2,4-dihydro-3H-pyrazole-3-one
2,5-Dimethyl-2H-pyrazole-3(4H)-one
[EINECS(EC#)]

220-389-2
[Molecular Formula]

C5H8N2O
[MDL Number]

MFCD00067008
[Molecular Weight]

112.13
[MOL File]

2749-59-9.mol
Chemical PropertiesBack Directory
[Melting point ]

117°C
[Boiling point ]

210.05°C (rough estimate)
[density ]

1.1524 (rough estimate)
[refractive index ]

1.4730 (estimate)
[storage temp. ]

Sealed in dry,Room Temperature
[solubility ]

Chloroform (Slightly), DMSO (Slightly), Ethyl Acetate (Slightly, Sonicated), Met
[form ]

Solid
[pka]

2.93±0.50(Predicted)
[color ]

Off-White to Light Beige
[Water Solubility ]

almost transparency
[InChI]

InChI=1S/C5H8N2O/c1-4-3-5(8)7(2)6-4/h3H2,1-2H3
[InChIKey]

JXPVQFCUIAKFLT-UHFFFAOYSA-N
[SMILES]

N1=C(C)CC(=O)N1C
[CAS DataBase Reference]

2749-59-9(CAS DataBase Reference)
[NIST Chemistry Reference]

3H-Pyrazol-3-one, 2,4-dihydro-2,5-dimethyl-(2749-59-9)
[EPA Substance Registry System]

3H-Pyrazol-3-one, 2,4-dihydro-2,5-dimethyl- (2749-59-9)
Safety DataBack Directory
[Hazard Codes ]

Xi
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
[Hazard Note ]

Irritant
[HS Code ]

2933199090
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Ethyl acetoacetate-->Acetyl ketene-->Methylhydrazine
[Preparation Products]

Fenpyroximate-->5-Chloro-1,3-dimethyl-1H-pyrazole-4-carbaldehyde-->Pyrazole-1,3-dimethyl-5-phenoxy-4-carboxaldehyde oxime
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

1,3-Dimethyl-5-pyrazolone(2749-59-9).msds
Hazard InformationBack Directory
[Chemical Properties]

Light Beige Solid
[Uses]

1,3-Dimethyl-5-pyrazolone (cas# 2749-59-9) is a compound useful in organic synthesis.
[Synthesis]

Ethyl acetoacetate

141-97-9

Methylhydrazine

60-34-4

1,3-Dimethyl-5-pyrazolone

2749-59-9

Methylhydrazine (4.47 mL, 84.99 mmol) was added slowly and dropwise to a solution of ethyl 3-oxohexanoate (11.06 g, 84.99 mmol) in anhydrous ethanol (100 mL) at 0 °C. The reaction system was naturally warmed to room temperature with continuous stirring for 3.5 hours. Subsequently, the reaction mixture was heated to 60 °C and the reaction was continued for 10 hours and kept at reflux for 2.5 hours. Upon completion of the reaction, the mixture was concentrated to dryness using a rotary evaporator to afford intermediate 4 as a viscous pink solid (9.52 g, 100% yield). The structure of intermediate 4 was confirmed by 1H NMR (400 MHz, CDCl3) and mass spectrometry (ESI): 1H NMR (400 MHz, CDCl3) δ (ppm): 5.06 (s, 1H), 3.85 (bs, 1H), 3.32 (s, 3H), 1.94 (s, 3H); MS (ESI): m/z calculated value ( C15H9N2O) was 113.1 and the measured value was 113.2 ([M+H]+).

[References]

[1] Bioorganic and Medicinal Chemistry Letters, 2005, vol. 15, # 13, p. 3307 - 3312
[2] Patent: WO2016/205460, 2016, A1. Location in patent: Paragraph 0140-0141
[3] Patent: WO2016/7905, 2016, A1. Location in patent: Page/Page column 37
[4] Bioorganic and Medicinal Chemistry Letters, 2016, vol. 26, # 23, p. 5815 - 5818
[5] Patent: US4382948, 1983, A
Spectrum DetailBack Directory
[Spectrum Detail]

1,3-Dimethyl-5-pyrazolone(2749-59-9)MS
1,3-Dimethyl-5-pyrazolone(2749-59-9)1HNMR
1,3-Dimethyl-5-pyrazolone(2749-59-9)13CNMR
1,3-Dimethyl-5-pyrazolone(2749-59-9)IR1
1,3-Dimethyl-5-pyrazolone(2749-59-9)IR2
Well-known Reagent Company Product InformationBack Directory
[TCI AMERICA]

1,3-Dimethyl-5-pyrazolone,>95.0%(LC)(T)(2749-59-9)
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