2-乙酰氨基苯甲醚(93-26-5)紅外圖譜(IR2)
InChI:InChI=1S/C9H11NO2/c1-7(11)10-8-5-3-4-6-9(8)12-2/h3-6H,1-2H3,(H,10,11)
InChIKey: FGOFNVXHDGQVBG-UHFFFAOYSA-N
Smiles:C(NC1=CC=CC=C1OC)(=O)C
-
Mass
MS-NW-1552
2'-methoxyacetanilide
C9H11NO2 (Mass of molecular ion: 165)
Source Temperature: 250 °C
Sample Temperature: 170 °C
Reservoir, 75 eV
15.0 7.4
26.0 1.1
27.0 2.4
28.0 1.8
38.0 2.3
39.0 5.9
41.0 2.6
42.0 1.6
43.0 29.0
50.0 3.6
51.0 9.0
52.0 15.1
53.0 6.8
54.0 1.2
62.0 1.3
63.0 4.4
64.0 3.0
65.0 14.8
66.0 2.3
76.0 1.1
77.0 4.1
78.0 4.2
79.0 3.6
80.0 43.0
81.0 2.7
91.0 1.8
92.0 8.0
93.0 3.2
94.0 3.9
95.0 2.3
106.0 1.5
108.0 100.0
109.0 7.7
120.0 1.8
122.0 1.3
123.0 74.4
124.0 6.2
134.0 1.4
165.0 48.3
166.0 5.2
400 MHz in CDCl3
90 MHz in CDCl3
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| 1H NMR |
399.65 MHz |
| C9 H11 N O2
|
0.042 g : 0.5 ml CDCl3
|
| 2'-methoxyacetanilide
|
 |
Assign. Shift(ppm)
A 8.346
B 7.80
C 7.018
D 6.940
E 6.856
F 3.853
G 2.179
C AND D WERE CONFIRMED BY LAOCN PROGRAM.
|
Hz ppm Int.
3340.45 8.359 56
3338.87 8.355 57
3332.52 8.339 59
3330.93 8.335 58
2806.88 7.024 62
2805.30 7.020 60
2799.07 7.004 52
2797.36 7.000 49
2781.37 6.960 66
2780.88 6.959 66
2779.91 6.956 76
2779.42 6.955 71
2773.32 6.940 98
2771.97 6.936 105
2765.87 6.921 45
2765.38 6.920 47
2764.40 6.918 45
2763.92 6.916 41
2744.38 6.867 93
2743.04 6.864 85
2736.33 6.847 71
2734.99 6.844 66
1540.16 3.854 1000
870.97 2.180 664
-
| 1H NMR |
89.56 MHz |
| C9 H11 N O2
|
0.035 g : 0.5 ml CDCl3
|
| 2'-methoxyacetanilide
|
|
Assign. Shift(ppm)
A 2.181
B 3.861
C 6.77 to 7.15
D 7.8
E 8.34
|
Hz ppm Int.
742.13 8.287 32
632.25 7.060 40
628.75 7.021 45
628.44 7.017 41
625.81 6.988 127
625.38 6.983 132
622.81 6.955 94
621.63 6.941 45
619.06 6.913 97
617.25 6.893 100
614.63 6.863 48
614.13 6.858 47
345.81 3.862 1000
195.31 2.181 991