2-萘甲醚(93-04-9)紅外圖譜(IR2)
InChI:InChI=1S/C11H10O/c1-12-11-7-6-9-4-2-3-5-10(9)8-11/h2-8H,1H3
InChIKey: LUZDYPLAQQGJEA-UHFFFAOYSA-N
Smiles:C1=C2C(C=CC=C2)=CC=C1OC
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Mass
MS-NW-4387
2-methoxynaphthalene
C11H10O (Mass of molecular ion: 158)
Source Temperature: 220 °C
Sample Temperature: 170 °C
Reservoir, 75 eV
14.0 1.0
15.0 1.6
17.0 1.0
18.0 4.8
39.0 3.2
50.0 2.3
51.0 2.9
62.0 3.1
63.0 6.5
64.0 1.1
65.0 3.4
74.0 2.3
75.0 2.6
76.0 1.2
77.0 2.3
79.0 2.7
86.0 1.1
87.0 1.7
88.0 2.2
89.0 5.6
101.0 1.3
113.0 2.3
114.0 4.5
115.0 85.8
116.0 8.6
126.0 2.6
127.0 5.8
128.0 12.4
129.0 3.9
142.0 1.0
143.0 7.8
144.0 1.0
158.0 100.0
159.0 12.1
160.0 1.0
400 MHz in CDCl3
90 MHz in CDCl3
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| 1H NMR |
399.65 MHz |
| C11 H10 O
|
0.015 g : 0.5 ml CDCl3
|
| 2-methoxynaphthalene
|
 |
Assign. Shift(ppm)
A 7.76
B 7.74
C 7.74
D *1 7.436
E *1 7.333
F 7.14
G 7.13
J 3.913
|
Hz ppm Int.
3107.79 7.777 47
3107.18 7.775 57
3106.45 7.773 61
3106.08 7.773 56
3099.00 7.755 67
3098.39 7.753 67
3097.90 7.752 70
3097.05 7.750 54
3095.34 7.746 141
3094.85 7.744 136
3087.16 7.725 136
3086.67 7.724 142
2979.86 7.457 38
2978.76 7.454 36
2973.14 7.440 52
2971.80 7.437 77
2970.70 7.434 35
2964.84 7.419 43
2963.75 7.416 42
2937.87 7.352 58
2936.52 7.348 59
2931.03 7.334 47
2929.81 7.331 87
2928.47 7.328 55
2922.85 7.314 39
2921.75 7.311 36
2861.82 7.161 54
2859.13 7.155 106
2850.83 7.134 248
1563.72 3.913 1000
1561.52 3.908 48
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| 1H NMR |
89.56 MHz |
| C11 H10 O
|
0.045 g : 0.5 ml CDCl3
|
| 2-methoxynaphthalene
|
|
Assign. Shift(ppm)
A 7.74
B 7.70
C 7.70
D 7.42
E 7.34
F 7.15
G 7.08
J 3.865
|
Hz ppm Int.
694.81 7.759 144
690.44 7.710 84
688.00 7.683 135
685.19 7.651 179
672.06 7.505 25
670.13 7.483 35
665.25 7.428 87
663.69 7.411 62
660.56 7.376 90
658.00 7.348 131
655.56 7.320 54
652.75 7.289 56
651.19 7.271 55
646.19 7.216 24
644.13 7.193 67
641.69 7.165 128
637.25 7.116 102
634.50 7.085 206
346.13 3.865 1000