三乙基硅烷(617-86-7)質譜(MS)

產(chǎn)品名稱:三乙基硅烷

CAS:617-86-7

分子式:C6H16Si

分子量: 116.28

InChI:InChI=1S/C6H16Si/c1-4-7(5-2)6-3/h7H,4-6H2,1-3H3

InChIKey: AQRLNPVMDITEJU-UHFFFAOYSA-N

Smiles:[SiH](CC)(CC)CC

Mass

MS-NW-7689          
triethylsilane
C6H16Si             (Mass of molecular ion:    116)

   Source Temperature: 260 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      27.0       2.2
      28.0       1.0
      29.0       4.9
      31.0      10.1
      43.0       7.3
      44.0       1.3
      45.0       3.5
      53.0       1.6
      55.0       3.4
      56.0       2.1
      57.0       6.3
      58.0      10.5
      59.0     100.0
      60.0       7.6
      61.0       3.7
      73.0       1.0
      86.0      22.0
      87.0      87.5
      88.0       8.8
      89.0       3.3
     115.0       2.6
     116.0       3.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₁₆ Si	0.05 ml : 0.5 ml CDCl₃
triethylsilane

    Assign.     Shift(ppm)

      A             3.621
      B             0.980
      C             0.591
     
     J(A,C)=3.1HZ
     J(A,SI-29)=-177HZ

     Hz     ppm     Int.

   1453.49   3.637     43
   1450.32   3.629     97
   1447.14   3.622    126
   1444.09   3.614     98
   1440.92   3.606     43
    411.74   1.031     36
    403.81   1.011     83
    399.41   1.000    509
    395.02   0.989    107
    391.24   0.979   1000
    388.06   0.971    101
    383.54   0.960    649
    379.39   0.950     68
    248.66   0.623    139
    245.61   0.615    151
    241.09   0.604    343
    237.92   0.596    347
    233.15   0.584    330
    229.98   0.576    330
    225.34   0.564    108
    224.85   0.563    112
    221.80   0.555    105

in CDCl3