N-乙酰-1-萘胺(575-36-0)核磁圖(¹HNMR)

產(chǎn)品名稱:N-乙酰-1-萘胺

CAS:575-36-0

分子式:C12H11NO

分子量: 185.22

InChI:InChI=1S/C12H11NO/c1-9(14)13-12-8-4-6-10-5-2-3-7-11(10)12/h2-8H,1H3,(H,13,14)

InChIKey: OKQIEBVRUGLWOR-UHFFFAOYSA-N

Smiles:C(NC1=C2C(C=CC=C2)=CC=C1)(=O)C

Mass

MS-NW-0410          
1-acetamidonaphthalene
C12H11NO            (Mass of molecular ion:    185)

   Source Temperature: 170 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      39.0       1.6
      43.0      10.0
      51.0       1.2
      62.0       1.1
      63.0       2.7
      65.0       1.2
      75.0       1.0
      88.0       1.1
      89.0       2.7
     113.0       1.4
     114.0       2.3
     115.0      21.8
     116.0       7.2
     117.0       1.1
     127.0       1.2
     140.0       2.2
     141.0       1.2
     142.0       2.9
     143.0     100.0
     144.0      12.8
     185.0      40.5
     186.0       5.6

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₂ H₁₁ N O	0.037 g : 0.5 ml DMSO-d₆
1-acetamidonaphthalene

    Assign.     Shift(ppm)

      A             9.96
      B             8.110
      C             7.926
      D     *1      7.75
      E     *1      7.72
      F     *2      7.56
      G     *2      7.52
      J             7.489
      K             2.209

     Hz     ppm     Int.

   3980.71   9.961    137
   3244.78   8.120    117
   3243.26   8.116    120
   3235.93   8.097    133
   3172.61   7.939    146
   3169.71   7.932     90
   3165.59   7.921    153
   3163.45   7.916    148
   3100.13   7.758    156
   3091.43   7.736    278
   3083.19   7.715    171
   3027.04   7.575     50
   3025.51   7.571     67
   3020.48   7.558    170
   3018.80   7.554    166
   3016.51   7.548    195
   3013.61   7.541    327
   3010.56   7.533    176
   3008.73   7.529    170
   3007.05   7.525    161
   3000.03   7.507    214
   2992.25   7.488    260
   2984.31   7.468    131
    883.18   2.210   1000

DMSO-d6