536-78-7

3-乙基吡啶(536-78-7)紅外圖譜(IR1)

產(chǎn)品名稱:3-乙基吡啶

CAS:536-78-7

分子式:C7H9N

分子量: 107.15

InChI:InChI=1S/C7H9N/c1-2-7-4-3-5-8-6-7/h3-6H,2H2,1H3

InChIKey: MFEIKQPHQINPRI-UHFFFAOYSA-N

Smiles:C1=NC=CC=C1CC

¹HNMR

¹³CNMR

IR1

Mass

MS-KW-0244          
3-ethylpyridine
C7H9N               (Mass of molecular ion:    107)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      26.0       1.7
      27.0       6.4
      28.0       3.0
      37.0       1.5
      38.0       3.9
      39.0      18.7
      40.0       1.6
      41.0       2.2
      50.0       6.7
      51.0      12.7
      52.0       8.2
      52.5       1.1
      53.0       4.9
      54.0       1.3
      62.0       1.3
      63.0       4.6
      64.0       2.6
      65.0      34.5
      66.0       3.2
      74.0       1.0
      75.0       1.1
      76.0       1.0
      77.0       8.8
      78.0       7.4
      79.0      18.0
      80.0       4.2
      92.0     100.0
      93.0       7.0
     104.0       2.1
     105.0       1.1
     106.0      45.9
     107.0      81.3
     108.0       7.0

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₇H₉N	0.05 ml : 0.5 ml CDCl₃
3-ethylpyridine

    Assign.     Shift(ppm)

     A           8.459
     B           8.423
     C           7.475
     D           7.174
     E           2.623
     F           1.232

     Hz     ppm     Int.

   3382.57   8.462    192
   3380.86   8.457    191
   3370.24   8.431    136
   3368.78   8.427    142
   3365.48   8.419    140
   3363.90   8.415    141
   2994.51   7.491     87
   2992.80   7.487    127
   2992.19   7.485    126
   2990.48   7.481     89
   2986.70   7.471     99
   2984.99   7.467    140
   2984.38   7.465    141
   2982.67   7.461     97
   2874.39   7.190    124
   2873.66   7.189    127
   2869.51   7.178    125
   2868.78   7.176    127
   2866.58   7.171    114
   2865.85   7.169    116
   2861.82   7.159    107
   2861.09   7.157    110
   1059.82   2.651    118
   1052.25   2.633    320
   1044.56   2.613    325
   1036.87   2.594    126
    555.06   1.389      9
    500.13   1.251    625
    492.44   1.232   1000
    484.75   1.213    598
    428.23   1.072     11

¹H NMR	89.56 MHz
C₇ H₉ N	0.05 ml : 0.5 ml CDCl₃
3-ethylpyridine

    Assign.     Shift(ppm)

      A             8.44
      B             8.41
      C             7.46
      D             7.16
      E             2.617
      F             1.236

     Hz     ppm     Int.

    756.31   8.445    302
    751.75   8.394    154
    750.13   8.376    145
    674.88   7.536     66
    673.06   7.516     95
    672.50   7.509     87
    671.88   7.503     58
    671.44   7.498     56
    670.81   7.491     64
    667.06   7.449    116
    666.38   7.441    101
    665.31   7.429    161
    664.75   7.423    148
    663.63   7.410     88
    663.00   7.403     99
    647.00   7.225    145
    646.38   7.218    130
    644.75   7.200     30
    644.25   7.194     30
    642.31   7.172    135
    641.50   7.163    123
    639.25   7.138     94
    638.56   7.130     82
    634.56   7.086     82
    633.88   7.078     72
    633.75   7.077     72
    246.69   2.755     84
    239.25   2.672    265
    236.31   2.639     37
    231.63   2.587    299
    224.06   2.502    118
    117.94   1.317    488
    110.56   1.235   1000
    106.19   1.186     43
    102.81   1.148    367

in CDCl3