二乙基羥胺(3710-84-7)核磁圖(¹³CNMR)

產(chǎn)品名稱:二乙基羥胺

CAS:3710-84-7

分子式:C4H11NO

分子量: 89.14

InChI:InChI=1S/C4H11NO/c1-3-5(6)4-2/h6H,3-4H2,1-2H3

InChIKey: FVCOIAYSJZGECG-UHFFFAOYSA-N

Smiles:C(N(CC)O)C

Mass

MS-NW-1137          
N,N-diethylhydroxylamine
C4H11NO             (Mass of molecular ion:     89)

   Source Temperature: 240 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      14.0       1.7
      15.0      18.4
      17.0       7.3
      18.0      35.8
      19.0       6.9
      26.0      10.8
      27.0      51.8
      28.0      64.9
      29.0     100.0
      30.0      62.9
      31.0       1.6
      32.0       1.7
      38.0       1.0
      39.0       2.7
      40.0       5.3
      41.0      30.7
      42.0      58.9
      43.0       6.2
      44.0      27.7
      45.0       3.8
      46.0      67.0
      47.0       1.2
      52.0       1.2
      54.0       3.8
      55.0       6.4
      56.0      51.9
      57.0       3.8
      58.0      71.3
      59.0      21.0
      60.0       8.7
      68.0       1.6
      69.0       1.6
      70.0      10.3
      71.0      12.7
      72.0      15.0
      73.0      18.6
      74.0      76.6
      75.0       3.0
      87.0      41.9
      88.0      10.1
      89.0      23.8
      90.0       1.3

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₄ H₁₁ N O	0.04 ml : 0.5 ml CDCl₃
N,N-diethylhydroxylamine

    Assign.     Shift(ppm)

      A             7.
      B             2.723
      C             1.154

     Hz     ppm     Int.

    255.13   2.849     74
    248.06   2.770    295
    240.94   2.691    337
    234.06   2.614    111
    110.19   1.231    427
    103.13   1.152   1000
     95.94   1.072    337

in CDCl3