1-甲氧基萘(2216-69-5)核磁圖(1HNMR)
InChI:InChI=1S/C11H10O/c1-12-11-8-4-6-9-5-2-3-7-10(9)11/h2-8H,1H3
InChIKey: NQMUGNMMFTYOHK-UHFFFAOYSA-N
Smiles:C1(OC)=C2C(C=CC=C2)=CC=C1
-
Mass
MS-NW-5217
methyl 1-naphthyl ether
C11H10O (Mass of molecular ion: 158)
Source Temperature: 260 °C
Sample Temperature: 190 °C
Reservoir, 75 eV
15.0 1.6
28.0 1.1
39.0 4.3
50.0 2.7
51.0 3.4
62.0 3.5
63.0 8.1
64.0 1.5
65.0 4.1
74.0 3.0
75.0 3.7
76.0 1.5
77.0 2.7
79.0 2.4
86.0 1.5
87.0 2.1
88.0 2.2
89.0 6.8
101.0 1.4
113.0 2.4
114.0 4.0
115.0 79.7
116.0 8.1
126.0 2.7
127.0 5.4
128.0 4.9
129.0 2.2
143.0 35.6
144.0 4.3
157.0 2.0
158.0 100.0
159.0 11.7
90 MHz in CDCl3
400 MHz in CDCl3
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| 1H NMR |
89.56 MHz |
| C11 H10 O
|
0.031 g : 0.5 ml CDCl3
|
| methyl 1-naphthyl ether
|
 |
Assign. Shift(ppm)
A 8.260
B 7.765
C 7.59 to 7.31
D 6.776
E 3.963
|
Hz ppm Int.
744.88 8.318 35
744.31 8.311 48
741.75 8.283 31
740.44 8.268 32
738.25 8.244 55
735.13 8.209 43
734.50 8.202 58
701.94 7.838 39
701.25 7.830 40
698.38 7.798 61
696.25 7.775 47
694.44 7.754 51
692.31 7.731 75
691.63 7.723 70
675.75 7.546 32
675.19 7.539 30
672.06 7.505 208
669.06 7.471 110
668.44 7.464 108
666.13 7.438 85
665.31 7.429 100
663.00 7.403 302
662.44 7.397 195
660.50 7.375 105
660.06 7.371 102
658.56 7.354 35
657.38 7.341 189
611.19 6.825 70
608.19 6.791 48
605.38 6.760 54
602.44 6.727 52
355.06 3.965 1000
354.75 3.962 999
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| 1H NMR |
399.65 MHz |
| C11 H10 O
|
0.031 g : 0.5 ml CDCl3
|
| methyl 1-naphthyl ether
|
|
Assign. Shift(ppm)
A 8.263
B 7.742
C *1 7.43
D *1 7.43
E 7.372
F 7.309
G 6.694
J 3.863
J(F,G)=7.3HZ. J(E,G)=1.0HZ.
|
Hz ppm Int.
3307.62 8.277 50
3306.88 8.275 83
3306.15 8.273 55
3304.69 8.269 43
3303.71 8.267 44
3303.10 8.265 48
3302.37 8.264 47
3300.90 8.260 69
3300.17 8.258 71
3297.85 8.252 52
3297.12 8.251 84
3296.39 8.249 53
3098.88 7.754 75
3095.70 7.747 89
3093.38 7.741 61
3092.04 7.737 50
3091.67 7.736 51
3089.36 7.731 83
2976.68 7.449 45
2975.95 7.447 40
2972.78 7.439 286
2969.85 7.432 149
2969.12 7.430 147
2966.92 7.424 136
2965.94 7.422 133
2963.13 7.415 259
2960.08 7.407 30
2959.11 7.405 35
2952.03 7.387 63
2951.29 7.385 87
2943.73 7.366 113
2942.99 7.364 148
2927.49 7.326 167
2919.92 7.307 175
2919.19 7.305 114
2911.62 7.286 99
2679.44 6.705 113
2678.59 6.703 113
2671.88 6.686 105
2671.02 6.684 104
1543.82 3.863 1000