3-(1-哌啶基)-丙酸乙酯(19653-33-9)核磁圖(¹HNMR)

產(chǎn)品名稱:3-(1-哌啶基)-丙酸乙酯

CAS:19653-33-9

分子式:C10H19NO2

分子量: 185.26

InChI:InChI=1S/C10H19NO2/c1-2-13-10(12)6-9-11-7-4-3-5-8-11/h2-9H2,1H3

InChIKey: MPAWVDTVWPPKJQ-UHFFFAOYSA-N

Smiles:N1(CCC(OCC)=O)CCCCC1

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-9828          
ethyl 1-piperidinepropionate
C10H19NO2           (Mass of molecular ion:    185)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      26.0       1.2
      27.0       7.3
      28.0       6.5
      29.0       7.9
      30.0       3.5
      39.0       1.8
      41.0       7.3
      42.0       9.7
      43.0       4.0
      44.0       5.2
      45.0       2.4
      54.0       2.1
      55.0      22.4
      56.0       8.0
      57.0       3.2
      58.0       1.1
      69.0       2.5
      70.0       3.4
      73.0       1.9
      82.0       1.3
      83.0       1.0
      84.0      10.5
      85.0       4.2
      96.0       4.9
      98.0     100.0
      99.0       7.8
     140.0       1.4
     156.0       2.1
     184.0       1.5
     185.0       4.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₁₉ N O₂	0.05 ml : 0.5 ml CDCl₃
ethyl 1-piperidinepropionate

    Assign.     Shift(ppm)

      A             4.133
      B             2.662
      C             2.497
      D             2.40
      E             1.570
      F             1.422
      G             1.255

     Hz     ppm     Int.

   1662.48   4.160    189
   1655.40   4.143    501
   1648.19   4.125    504
   1641.11   4.107    186
   1071.53   2.682    186
   1070.80   2.680    200
   1066.65   2.669     82
   1063.96   2.663    412
   1062.62   2.659    259
   1059.81   2.652     75
   1056.03   2.643    315
   1004.64   2.514    324
   1001.22   2.506     84
    996.95   2.495    420
    990.11   2.478    198
    989.50   2.476    199
    958.01   2.398    300
    639.40   1.600    142
    633.67   1.586    304
    627.93   1.572    432
    622.31   1.558    362
    616.94   1.544    160
    580.20   1.452     84
    573.97   1.437    150
    568.60   1.423    167
    564.70   1.413    106
    557.37   1.395     43
    508.91   1.274    569
    501.71   1.256   1000
    494.63   1.238    554

in CDCl3