2-氯乙醇亞磷酸鹽(3:1)(140-08-9)紅外圖譜(IR1)

產(chǎn)品名稱:2-氯乙醇亞磷酸鹽(3:1)

CAS:140-08-9

分子式:C6H12Cl3O3P

分子量: 269.49

InChI:InChI=1S/C6H12Cl3O3P/c7-1-4-10-13(11-5-2-8)12-6-3-9/h1-6H2

InChIKey: LUVCTYHBTXSAMX-UHFFFAOYSA-N

Smiles:P(OCCCl)(OCCCl)OCCCl

Mass

MS-NW-8328          
tris(2-chloroethyl) phosphite
C6H12Cl3O3P         (Mass of molecular ion:    268)

   Source Temperature: 260 °C
   Sample Temperature: 130 °C
   Reservoir, 75 eV

      15.0       2.1
      26.0       2.5
      27.0      44.6
      28.0      14.2
      29.0       2.4
      31.0      13.0
      36.0       2.1
      43.0       3.2
      44.0       1.6
      45.0       5.0
      47.0       8.0
      49.0       3.7
      51.0       1.3
      62.0      12.6
      63.0     100.0
      64.0       6.2
      65.0      42.6
      77.0       3.2
      81.0       1.7
      82.0       2.4
      83.0      14.7
      91.0       8.3
     109.0      11.8
     110.0       2.0
     117.0       4.7
     119.0       1.6
     127.0      13.5
     129.0       4.6
     135.0       2.2
     143.0       2.3
     145.0      18.7
     147.0       6.5
     171.0      18.8
     173.0       6.2
     189.0      32.5
     190.0       1.5
     191.0      20.8
     193.0       3.5
     207.0      17.0
     209.0      10.9
     211.0       1.8
     233.0      29.9
     234.0       2.1
     235.0      19.3
     236.0       1.3
     237.0       3.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₁₂ Cl₃ O₃ P	0.05 ml : 0.5 ml CDCl₃
tris(2-chloroethyl) phosphite

    Assign.     Shift(ppm)

      A             4.108
      B             3.677

     Hz     ppm     Int.

   1655.52   4.143     38
   1651.61   4.133    480
   1649.05   4.127     81
   1646.12   4.119    694
   1645.26   4.117    459
   1643.92   4.114    508
   1640.14   4.104    561
   1638.43   4.100    661
   1637.57   4.098    442
   1635.01   4.092     72
   1632.32   4.085    505
   1479.86   3.703     47
   1475.22   3.692    816
   1469.24   3.677   1000
   1463.50   3.662    695

in CDCl3