乙基氯苯胺(13519-75-0)核磁圖(¹HNMR)

產(chǎn)品名稱(chēng):乙基氯苯胺

CAS:13519-75-0

分子式:C8H10ClN

分子量: 155.62

InChI:InChI=1S/C8H10ClN/c1-2-10-8-5-3-7(9)4-6-8/h3-6,10H,2H2,1H3

InChIKey: KLWDPIXDUVYHMS-UHFFFAOYSA-N

Smiles:C1(NCC)=CC=C(Cl)C=C1

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-4738          
p-chloro-N-ethylaniline
C8H10ClN            (Mass of molecular ion:    155)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      28.0       1.1
      39.0       1.0
      50.0       1.3
      51.0       1.4
      52.0       1.1
      63.0       1.8
      64.0       1.0
      65.0       2.0
      70.0       4.3
      71.0       1.4
      73.0       1.2
      75.0       4.7
      76.0       1.1
      77.0       8.4
      78.0       1.2
      90.0       1.0
      91.0       2.1
      92.0       1.5
      99.0       2.8
     101.0       1.0
     104.0       3.3
     105.0       6.6
     111.0       5.2
     112.0       3.4
     113.0       3.0
     114.0       1.2
     117.0       1.0
     118.0       4.1
     119.0       3.6
     127.0       1.1
     138.0       2.1
     140.0     100.0
     141.0       8.5
     142.0      32.3
     143.0       2.6
     154.0       4.5
     155.0      40.3
     156.0       5.2
     157.0      13.1
     158.0       1.2
     168.0       1.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₁₀ Cl N	0.05 ml : 0.5 ml CDCl₃
p-chloro-N-ethylaniline

    Assign.     Shift(ppm)

      A             7.073
      B             6.446
      C             3.50
      D             3.034
      E             1.176

     Hz     ppm     Int.

   2834.59   7.093     83
   2831.42   7.085    660
   2829.10   7.079    221
   2824.71   7.068    242
   2822.39   7.063    646
   2819.21   7.055     92
   2583.62   6.465     77
   2580.44   6.457    589
   2578.13   6.451    194
   2573.73   6.440    197
   2571.53   6.435    528
   2568.24   6.427     70
   1397.46   3.497     33
   1223.51   3.062    169
   1216.31   3.044    459
   1209.23   3.026    463
   1202.03   3.008    180
    476.93   1.194    612
    469.85   1.176   1000
    462.65   1.158    576

in CDCl3