118-31-0

1-萘甲基胺(118-31-0)核磁圖(¹HNMR)

產(chǎn)品名稱:1-萘甲基胺

CAS:118-31-0

分子式:C11H11N

分子量: 157.21

InChI:InChI=1S/C11H11N/c12-8-10-6-3-5-9-4-1-2-7-11(9)10/h1-7H,8,12H2

InChIKey: NVSYANRBXPURRQ-UHFFFAOYSA-N

Smiles:C1(CN)=C2C(C=CC=C2)=CC=C1

Mass

MS-NW-5568          
((1-naphthyl)methyl)amine
C11H11N             (Mass of molecular ion:    157)

   Source Temperature: 250 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      18.0       1.7
      28.0       7.1
      29.0       1.7
      30.0      15.6
      39.0       2.7
      50.0       3.0
      51.0       5.0
      52.0       1.2
      62.0       1.9
      63.0       5.0
      64.0       2.1
      65.0       2.7
      74.0       3.1
      75.0       3.8
      76.0       2.6
      76.5       2.2
      77.0       8.1
      77.5       4.8
      78.0       4.5
      78.5       3.5
      86.0       1.0
      87.0       1.5
      89.0       1.9
      91.0       1.0
      98.0       1.1
     101.0       2.7
     102.0       3.0
     103.0       1.0
     113.0       1.0
     115.0       9.0
     116.0       1.1
     126.0       5.1
     127.0      16.6
     128.0      31.0
     129.0      41.6
     130.0       5.9
     139.0       7.7
     140.0       4.8
     141.0      19.6
     142.0       3.4
     153.0       3.8
     154.0       7.0
     155.0       2.7
     156.0     100.0
     157.0      93.8
     158.0      11.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₁₁ N	0.05 ml : 0.5 ml CDCl₃
((1-naphthyl)methyl)amine

    Assign.     Shift(ppm)

      A             7.945
      B             7.79
      C             7.679
      D     *1      7.45
      E     *1      7.41
      F             7.35
      G             7.34
      J             4.168
      K             1.77

     Hz     ppm     Int.

   3180.66   7.959    192
   3179.44   7.956    218
   3178.59   7.954    203
   3173.71   7.942    108
   3172.61   7.939    185
   3171.63   7.937    236
   3171.02   7.935    238
   3122.92   7.815     30
   3118.04   7.802    225
   3117.07   7.800    209
   3115.72   7.797    187
   3114.01   7.792    107
   3113.40   7.791    110
   3110.35   7.783    291
   3108.52   7.779    266
   3105.22   7.770     63
   3101.68   7.761     30
   3073.12   7.690    170
   3070.31   7.683    185
   3066.53   7.674    151
   3063.72   7.667    199
   2991.09   7.485     30
   2990.23   7.483     31
   2989.62   7.481     32
   2988.65   7.479     34
   2988.28   7.478     34
   2986.57   7.473     62
   2985.23   7.470    148
   2983.64   7.466    178
   2981.93   7.462     81
   2978.52   7.453    312
   2976.81   7.449    294
   2975.46   7.446    181
   2970.83   7.434    536
   2968.87   7.429    502
   2966.43   7.423    143
   2964.11   7.417    177
   2963.01   7.415    274
   2961.55   7.411    300
   2959.35   7.405    112
   2958.01   7.402    119
   2956.18   7.397    169
   2954.71   7.394    131
   2952.76   7.389     48
   2951.90   7.387     47
   2951.66   7.386     47
   2950.81   7.384     47
   2950.32   7.383     46
   2949.95   7.382     46
   2949.46   7.381     45
   2948.73   7.379     46
   2948.36   7.378     45
   2948.12   7.377     45
   2946.04   7.372    153
   2938.96   7.354    498
   2934.94   7.344    374
   2932.25   7.338   1000
   2927.98   7.327    122
   1665.77   4.169    623
   1653.44   4.138     33
   1652.83   4.136     33
   1652.47   4.135     33
    707.89   1.772    181

in CDCl3