6-氟-2-甲基喹啉(1128-61-6)核磁圖(¹HNMR)

產(chǎn)品名稱:6-氟-2-甲基喹啉

CAS:1128-61-6

分子式:C10H8FN

分子量: 161.18

InChI:InChI=1S/C10H8FN/c1-7-2-3-8-6-9(11)4-5-10(8)12-7/h2-6H,1H3

InChIKey: GPIARMSVZOEZCV-UHFFFAOYSA-N

Smiles:N1C2C(=CC(F)=CC=2)C=CC=1C

Mass

MS-IW-3641          
6-fluoro-2-methylquinoline
C10H8FN             (Mass of molecular ion:    161)

   Source Temperature: 230 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      39.0       1.2
      50.0       1.6
      51.0       1.2
      57.0       1.7
      63.0       1.5
      66.5       1.0
      67.5       2.4
      74.0       1.7
      75.0       2.0
      79.5       1.2
      80.5       3.3
      81.0       1.7
      93.0       1.3
      94.0       3.4
      95.0       1.5
      99.0       2.7
     100.0       1.0
     107.0       3.0
     108.0       2.1
     119.0       2.9
     120.0       1.6
     126.0       3.5
     131.0       1.0
     132.0       1.3
     133.0      15.3
     134.0       7.1
     135.0       3.5
     140.0       1.2
     146.0      12.5
     147.0       1.3
     158.0       2.5
     159.0       1.4
     160.0      15.3
     161.0     100.0
     162.0      11.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₈ F N	0.053 g : 0.5 ml CDCl₃
6-fluoro-2-methylquinoline

    Assign.     Shift(ppm)

      A             7.996
      B             7.943
      C             7.429
      D             7.345
      E             7.260
      F             2.715

     Hz     ppm     Int.

   3203.37   8.016     88
   3198.12   8.003     91
   3194.21   7.993     99
   3188.84   7.980     98
   3178.34   7.953    167
   3169.92   7.932    176
   2979.13   7.455     76
   2976.32   7.448     87
   2970.70   7.434     89
   2969.97   7.432     84
   2967.90   7.427    104
   2967.16   7.425     99
   2961.55   7.411     70
   2958.74   7.404     83
   2941.41   7.360    121
   2938.60   7.353    105
   2932.62   7.338    122
   2929.69   7.331    106
   2906.01   7.272    162
   2905.52   7.271    163
   2897.58   7.251    153
   2896.97   7.249    156
   1085.08   2.716   1000

in CDCl3