3-甲基-2-苯基吡啶(10273-90-2)核磁圖(¹HNMR)

產(chǎn)品名稱:3-甲基-2-苯基吡啶

CAS:10273-90-2

分子式:C12H11N

分子量: 169.22

InChI:InChI=1S/C12H11N/c1-10-6-5-9-13-12(10)11-7-3-2-4-8-11/h2-9H,1H3

InChIKey: BJATUPPYBZHEIO-UHFFFAOYSA-N

Smiles:C1(C2=CC=CC=C2)=NC=CC=C1C

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-9294          
3-methyl-2-phenylpyridine
C12H11N             (Mass of molecular ion:    169)

   Source Temperature: 240 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      39.0       6.3
      40.0       1.3
      50.0       1.4
      51.0       3.2
      63.0       3.1
      64.0       1.5
      65.0       3.0
      70.5       1.8
      71.5       1.5
      76.0       1.6
      77.0       3.9
      83.5      10.5
      84.0       2.7
      84.5       1.7
      89.0       1.4
     115.0       3.4
     139.0       2.5
     140.0       2.4
     141.0       3.0
     166.0       4.0
     167.0      24.8
     168.0     100.0
     169.0      30.0
     170.0       3.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₂ H₁₁ N	0.05 ml : 0.5 ml CDCl₃
3-methyl-2-phenylpyridine

    Assign.     Shift(ppm)

      A             8.509
      B             7.51
      C             7.418
      D             7.359
      E             7.119
      F             2.310

     Hz     ppm     Int.

   3404.17   8.518    120
   3403.81   8.517    121
   3402.59   8.514    128
   3399.41   8.506    124
   3399.05   8.506    125
   3397.83   8.503    128
   3009.16   7.530    154
   3006.84   7.524    245
   3005.13   7.520    304
   3002.93   7.514    145
   3001.46   7.511    172
   2999.88   7.507    267
   2998.17   7.502    377
   2997.07   7.500    329
   2995.12   7.495     72
   2973.39   7.440    122
   2971.92   7.437    195
   2970.09   7.432     84
   2966.67   7.424    105
   2964.84   7.419    366
   2963.26   7.415    196
   2958.74   7.404    121
   2957.52   7.401    218
   2957.03   7.400    212
   2955.44   7.396     54
   2947.39   7.375    103
   2945.92   7.372    180
   2944.46   7.368    106
   2941.16   7.360     68
   2938.84   7.354    183
   2936.04   7.347     46
   2932.74   7.339     42
   2931.40   7.335     63
   2930.18   7.332     34
   2851.07   7.134    163
   2846.31   7.123    160
   2843.38   7.115    149
   2838.62   7.103    147
    923.46   2.311   1000

in CDCl3