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ChemicalBook--->CAS DataBase List--->775-00-8

775-00-8

775-00-8 Structure

775-00-8 Structure
IdentificationMore
[Name]

2-(4-TRIFLUOROMETHYL-PHENYL)-ETHYLAMINE
[CAS]

775-00-8
[Synonyms]

2-[4-(TRIFLUOROMETHYL)PHENYL]ETHANAMINE
2-(4-TRIFLUOROMETHYL-PHENYL)-ETHYLAMINE
RARECHEM AL BW 0217
4-Trifluoromethylphenethylamine
[Molecular Formula]

C9H10F3N
[MDL Number]

MFCD01529875
[Molecular Weight]

189.18
[MOL File]

775-00-8.mol
Chemical PropertiesBack Directory
[Boiling point ]

210℃
[density ]

1.186
[refractive index ]

1.4620 to 1.4660
[Fp ]

86℃
[storage temp. ]

under inert gas (nitrogen or Argon) at 2–8 °C
[form ]

clear liquid
[pka]

9.49±0.10(Predicted)
[color ]

Colorless to Light yellow to Light orange
[Water Solubility ]

Slightly soluble in water.
[InChI]

InChI=1S/C9H10F3N/c10-9(11,12)8-3-1-7(2-4-8)5-6-13/h1-4H,5-6,13H2
[InChIKey]

HMFOBPNVAAAACP-UHFFFAOYSA-N
[SMILES]

C1(CCN)=CC=C(C(F)(F)F)C=C1
[CAS DataBase Reference]

775-00-8(CAS DataBase Reference)
Safety DataBack Directory
[RIDADR ]

UN 2735 8/PG II
[HazardClass ]

8
[HazardClass ]

IRRITANT
[PackingGroup ]

II
[HS Code ]

2921490090
Hazard InformationBack Directory
[Uses]

It is applied as an active pharmaceutical intermediate.
[Synthesis]

4-(TRIFLUOROMETHYL)PHENYLACETONITRILE

2338-75-2

2-(4-TRIFLUOROMETHYL-PHENYL)-ETHYLAMINE

775-00-8

The general procedure for the synthesis of 2-(4-trifluoromethylphenyl)ethylamine from p-trifluoromethylphenylacetonitrile was as follows: (4-trifluoromethylphenyl)acetonitrile (2 g, 10.81 mmol) was dissolved in methanol-ammonia solution (50 mL), which was subsequently added to a Parr hydrogenation reactor that had been charged with nickel Nguyenay (400 mg). The reaction mixture was stirred overnight under hydrogen pressure of 50 psi. The progress of the reaction was monitored by thin layer chromatography (TLC, the unfolding agent was a chloroform solution containing 10% methanol). Upon completion of the reaction, the mixture was filtered through a bed of diatomaceous earth and the filtrate was concentrated and dried under reduced pressure to afford the target product 2-(4-trifluoromethylphenyl)ethylamine (2 g, 97.89% yield). The product was analyzed by LCMS and the purity was 98.73%, m/z = 190.0 ([M+H]+).

[References]

[1] Patent: WO2012/35078, 2012, A1. Location in patent: Page/Page column 67
[2] Patent: US2014/45872, 2014, A1. Location in patent: Paragraph 0403
[3] Patent: WO2004/82682, 2004, A1. Location in patent: Page 44-45
[4] Patent: WO2003/93231, 2003, A2. Location in patent: Page/Page column 48
[5] Patent: WO2005/80371, 2005, A1. Location in patent: Page/Page column 49
Spectrum DetailBack Directory
[Spectrum Detail]

2-(4-TRIFLUOROMETHYL-PHENYL)-ETHYLAMINE(775-00-8)1HNMR
Well-known Reagent Company Product InformationBack Directory
[Sigma Aldrich]

775-00-8(sigmaaldrich)
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