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ChemicalBook--->CAS DataBase List--->6343-93-7

6343-93-7

6343-93-7 Structure

6343-93-7 Structure
IdentificationMore
[Name]

4-METHOXYPHENYLACETAMIDE
[CAS]

6343-93-7
[Synonyms]

2-(4-METHOXY-PHENYL)-ACETAMIDE
4-METHOXYPHENYLACETAMIDE
PARA METHOXYL PHENYL ACETAMIDE
PARA METHOXYPHENYL ACETAMIDE
P-METHOXYPHENYLACETAMIDE
Benzeneacetamide, 4-methoxy-
4-Methoxybenzeneacetamide
[EINECS(EC#)]

228-745-9
[Molecular Formula]

C9H11NO2
[MDL Number]

MFCD00017144
[Molecular Weight]

165.19
[MOL File]

6343-93-7.mol
Chemical PropertiesBack Directory
[Melting point ]

182-184°C
[Boiling point ]

354.7±25.0 °C(Predicted)
[density ]

1.123±0.06 g/cm3(Predicted)
[storage temp. ]

Sealed in dry,Room Temperature
[solubility ]

DMSO (Slightly), Methanol (Slightly)
[form ]

Solid
[pka]

16.37±0.40(Predicted)
[color ]

White to Off-White
[BRN ]

2088040
[CAS DataBase Reference]

6343-93-7(CAS DataBase Reference)
Safety DataBack Directory
[Safety Statements ]

S22:Do not breathe dust .
S24/25:Avoid contact with skin and eyes .
[HS Code ]

2924297099
Hazard InformationBack Directory
[Uses]

4-Methoxyphenylacetamide is a useful reagent in the preparation of novel pyrrolidone-??based derivatives as potential p53-??MDM2 inhibitors for use as potential antitumor agents.
[Synthesis]

4-Methoxybenzyl cyanide

104-47-2

4-METHOXYPHENYLACETAMIDE

6343-93-7

General procedure for the synthesis of 4-methoxybenzeneacetamide from p-methoxybenzeneacetonitrile: Ni NPs/HT catalyst (0.05 g) was added to a thick-walled pressure tube, followed by water (4 ml) and p-methoxybenzeneacetonitrile (1 mmol). The reaction mixture was placed in an oil bath at 120 °C and stirred vigorously. The reaction process was monitored by TLC analysis. Upon completion of the reaction, the reaction mixture was extracted with ethyl acetate and subsequently filtered to remove the catalyst. The filtrate was cooled to 0 °C to allow white crystals to precipitate. The crystalline product was collected by simple filtration and dried under vacuum at room temperature to give analytically pure 4-methoxyphenylacetamide. If the product did not precipitate, the reaction mixture was extracted with ethyl acetate followed by purification by silica gel column chromatography to finally obtain 4-methoxyphenylacetamide.

[References]

[1] Synthesis, 1989, # 12, p. 949 - 951
[2] RSC Advances, 2015, vol. 5, # 9, p. 6365 - 6371
[3] Zeitschrift fur Chemie, 1980, vol. 20, # 10, p. 380 - 380
[4] Catalysis Communications, 2012, vol. 29, p. 109 - 113
[5] Green Chemistry, 2014, vol. 16, # 4, p. 2136 - 2141
Spectrum DetailBack Directory
[Spectrum Detail]

4-METHOXYPHENYLACETAMIDE(6343-93-7)MS
4-METHOXYPHENYLACETAMIDE(6343-93-7)1HNMR
4-METHOXYPHENYLACETAMIDE(6343-93-7)IR1
4-METHOXYPHENYLACETAMIDE(6343-93-7)IR2
Well-known Reagent Company Product InformationBack Directory
[Alfa Aesar]

4-Methoxyphenylacetamide, 98%(6343-93-7)
[Sigma Aldrich]

6343-93-7(sigmaaldrich)
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