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ChemicalBook--->CAS DataBase List--->2298-07-9

2298-07-9

2298-07-9 Structure

2298-07-9 Structure
IdentificationMore
[Name]

4-Bromo-1-naphthylamine
[CAS]

2298-07-9
[Synonyms]

1-AMINO-4-BROMONAPHTHALENE
4-BROMO-1-NAPHTHALENAMINE
4-BROMO-1-NAPHTHYLAMINE
1-Amino-4-bromoaphthlalene
1-Naphthalenamine, 4-bromo-
4-BROMO-1-NAPHTHALENYLAMINE
4-Bromo-1-naphtylamine
4-Bromonaphthalene-1-amine
[EINECS(EC#)]

218-944-9
[Molecular Formula]

C10H8BrN
[MDL Number]

MFCD00004023
[Molecular Weight]

222.08
[MOL File]

2298-07-9.mol
Chemical PropertiesBack Directory
[Melting point ]

102-103 °C(lit.)
[Boiling point ]

338.4±17.0 °C(Predicted)
[density ]

1.563±0.06 g/cm3(Predicted)
[storage temp. ]

Keep in dark place,Sealed in dry,Room Temperature
[form ]

powder to crystal
[pka]

2.93±0.10(Predicted)
[color ]

White to Amber to Dark purple
[InChI]

InChI=1S/C10H8BrN/c11-9-5-6-10(12)8-4-2-1-3-7(8)9/h1-6H,12H2
[InChIKey]

LIUKLAQDPKYBCP-UHFFFAOYSA-N
[SMILES]

C1(N)=C2C(C=CC=C2)=C(Br)C=C1
[CAS DataBase Reference]

2298-07-9(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

Xi,Xn
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
R20/21/22:Harmful by inhalation, in contact with skin and if swallowed .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S37/39:Wear suitable gloves and eye/face protection .
S36:Wear suitable protective clothing .
[WGK Germany ]

3
[Hazard Note ]

Irritant
[HS Code ]

29214990
Hazard InformationBack Directory
[Chemical Properties]

pale purple fibrous powder
[Uses]

1-Amino-4-bromonaphthalene is a reagent used in catalytic asymmetric ring opening of meso-epoxides with aromatic amines in water. It can also be used to synthesize of 4-quinolones and quinolone heterocycles.
[Synthesis]

4-Bromo-1-naphthylamine is synthesised using 1-(acetylamino)-4-bromonaphthalene as a raw material by chemical reaction. The specific synthesis steps are as follows:
The 4-bromo-1-acetamido naphthalene obtained in the first step is dissolved in 100 mL of 95% ethanol, and the mass concentration of 4-bromo-1-acetylaminonaphthalene in the mixed solution is 30%, and the mass concentration is 37% added to the mixed solution. 50mL of concentrated hydrochloric acid, reacted at 80 ° C for 6h, filtered and dried to give 4-bromo-1-naphthylamine.
4-Bromo-1-naphthylamine synthesis
Spectrum DetailBack Directory
[Spectrum Detail]

4-Bromo-1-naphthylamine(2298-07-9)MS
4-Bromo-1-naphthylamine(2298-07-9)1HNMR
4-Bromo-1-naphthylamine(2298-07-9)13CNMR
4-Bromo-1-naphthylamine(2298-07-9)IR1
4-Bromo-1-naphthylamine(2298-07-9)IR2
4-Bromo-1-naphthylamine(2298-07-9)Raman
Well-known Reagent Company Product InformationBack Directory
[Sigma Aldrich]

2298-07-9(sigmaaldrich)
[TCI AMERICA]

1-Amino-4-bromonaphthalene,>96.0%(T)(2298-07-9)
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