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ChemicalBook--->CAS DataBase List--->122-75-8

122-75-8

122-75-8 Structure

122-75-8 Structure
IdentificationMore
[Name]

N,N'-Dibenzyl ethylenediamine diacetate
[CAS]

122-75-8
[Synonyms]

1,2-DI(BENZYLAMINE)ETHANE DIACETATE
DBED-ACETATE
N,N'-DIBENZYLETHYLENEDIAMINE DIACETATE
N,N-DIBENZYLETHYLENEDIAMINE DIACETATE
2-ethanediamine,n,n’-bis(phenylmethyl)-diacetate
dbeddiacetate
n,n’-dibenzyl-ethylenediamindiacetate
N,N'-dibenzylethylenediammonium di(acetate)
N,N'-DIBENZYLETHYLENEDIAMINE DIACETATE (SYM.)
N,N-DibenzylethyleneDiamineAcetate
N,N'-DibenzylethylenediamineDiacetate>96%
N,N-Dibenzyl Ethylenediamine Diacetic Acid
1,2-Di-[benzylamino] ethane diacetate
N,N-Dibenzyl ethylenediamine dicetic acid
1,2-Ethanediamine, N,N-bis(phenylmethyl)-, diacetate
N,N-Dibenzyl-ethleBediamine diacetic acid
N''N-DIBENZYL-ETHYLENEDIAMINE DIACETIC ACID (DBED)
N,N''-DIBENZYLETHYLDIAMINEDIACETICACID
N,N'-Dibenzylethylenediamine·2acetic acid
[EINECS(EC#)]

204-572-4
[Molecular Formula]

C20H28N2O4
[MDL Number]

MFCD00040588
[Molecular Weight]

360.45
[MOL File]

122-75-8.mol
Chemical PropertiesBack Directory
[Melting point ]

117-118°C
[bulk density]

280kg/m3
[storage temp. ]

Store below +30°C.
[solubility ]

Chloroform (Slightly), Ethyl Acetate (Slightly), Water (Slightly)
[Water Solubility ]

Soluble in water
[form ]

powder to crystal
[color ]

White to Almost white
[PH]

5-6 (50g/l, H2O, 20°C)
[Merck ]

14,1064
[BRN ]

3781362
[InChI]

InChI=1S/C16H20N2.2C2H4O2/c1-3-7-15(8-4-1)13-17-11-12-18-14-16-9-5-2-6-10-16;2*1-2(3)4/h1-10,17-18H,11-14H2;2*1H3,(H,3,4)
[InChIKey]

MTRNNCLQPVCDLF-UHFFFAOYSA-N
[SMILES]

C1(=CC=CC=C1)CNCCNCC1=CC=CC=C1.C(=O)(O)C.C(=O)(O)C
[CAS DataBase Reference]

122-75-8(CAS DataBase Reference)
[EPA Substance Registry System]

122-75-8(EPA Substance)
Safety DataBack Directory
[Risk Statements ]

R22:Harmful if swallowed.
R43:May cause sensitization by skin contact.
[Safety Statements ]

S36/37:Wear suitable protective clothing and gloves .
[WGK Germany ]

WGK 3 highly water endangering
[RTECS ]

KV3400000
[TSCA ]

Yes
[HS Code ]

2921 59 90
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Benzaldehyde-->Ethylenediamine-->Acetic acid-->N,N'-Bis(phenylmethyl)-1,2-ethanediamine
Hazard InformationBack Directory
[Chemical Properties]

White needle crystal
[Uses]

N,N''-Dibenzylethylenediamine is currently being investigated as a potential hepatitis C virus inhibitor. N,N''-dibenzylethylenediamine and its derivatives are also inhibitors of cholesterol biosynthesis.
[Synthesis]

Acetic acid

64-19-7

N,N'-Bis(phenylmethyl)-1,2-ethanediamine

140-28-3

N,N'-Dibenzyl ethylenediamine diacetate

122-75-8

S3. The mixed organic phase of Compound C with toluene obtained in step S2 was transferred to a three-necked flask and the fractions were removed by distillation. After the mixture was cooled to 30°C, it was dissolved in 200 g of ethyl acetate and heated to 60°C. Subsequently, 20 g of glacial acetic acid at 98% concentration was slowly added dropwise. After the dropwise addition was completed, the reaction conditions were maintained for 1.0 hour. Upon completion of the reaction, the mixture was slowly cooled and 49.5 g of the wet product (i.e., a hydrate containing N,N'-dibenzylethylenediamine diacetate) was collected by filtration. The wet product was dried at 45 °C to give 49.0 g of N,N'-dibenzylethylenediamine diacetate (i.e., compound D).

[References]

[1] Patent: CN108558676, 2018, A. Location in patent: Page/Page column 8-10
Spectrum DetailBack Directory
[Spectrum Detail]

N,N'-Dibenzyl ethylenediamine diacetate(122-75-8)MS
N,N'-Dibenzyl ethylenediamine diacetate(122-75-8)1HNMR
N,N'-Dibenzyl ethylenediamine diacetate(122-75-8)13CNMR
N,N'-Dibenzyl ethylenediamine diacetate(122-75-8)IR1
N,N'-Dibenzyl ethylenediamine diacetate(122-75-8)Raman
Well-known Reagent Company Product InformationBack Directory
[Alfa Aesar]

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