Triphenylmethyl Chloride synthesis
- Product Name:Triphenylmethyl Chloride
- CAS Number:76-83-5
- Molecular formula:C19H15Cl
- Molecular Weight:278.78
76-84-6
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76-83-5
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Yield:76-83-5 100%
Reaction Conditions:
with Vilsmeier reagent in 1,4-dioxane at 80; for 0.5 h;
Steps:
212
0.44 g (3.4 mmol) of the crystal of N, N-dimethylchloromethyleneiminium chloride synthesized in Example I-101 was suspended in 10 mL of 1,4-dioxane, 0.72 g (2.00 mmol) 8 mmol) in 1,4-dioxane 4 mL was added dropwise at room temperature. When stirred at 80 ° C. for 30 minutes, a homogeneous solution was obtained. Sodium bicarbonate water and dichloromethane were added, the organic phase was separated, and the solvent was distilled off, whereby 0.78 g of triphenylmethyl chloride was obtained in a quantitative yield.
References:
JP5782331,2015,B2 Location in patent:Paragraph 0047
519-73-3
253 suppliers
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76-83-5
715 suppliers
$6.00/25g
