Tetrapropylammonium bromide synthesis
- Product Name:Tetrapropylammonium bromide
- CAS Number:1941-30-6
- Molecular formula:C12H28BrN
- Molecular Weight:266.27
102-69-2
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106-94-5
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$10.00/5ml
1941-30-6
473 suppliers
$7.00/25g
Yield:-
Reaction Conditions:
in N,N-dimethyl-formamide at 110; for 15 h;Inert atmosphere;
Steps:
General Procedure for the Synthesis of Tetrapropylammonium Bromide
A mixture of tripropylamine (1 mol) and propyl bromide (1.5 mol) in DMF (100mL) was stirred at 110 C for 15 h under an N2 atmosphere. After completion of reaction, the reaction mixture was cooled (ice-bath) and n-hexane/toluene (2 : 1)(200 mL) was added. The precipitate was filtered and washed with n-hexane/toluene (3 : 1) (40 mL) to give the desired TPAB
References:
Ezzati, Mahnaz;Khalafy, Jabbar;Marjani, Ahmad Poursattar;Prager, Rolf H. [Australian Journal of Chemistry,2018,vol. 71,# 6,p. 435 - 441]
106-94-5
577 suppliers
$10.00/5ml
1941-30-6
473 suppliers
$7.00/25g