N-(3-FORMYLPHENYL)METHANESULFONAMIDE synthesis
- Product Name:N-(3-FORMYLPHENYL)METHANESULFONAMIDE
- CAS Number:55512-05-5
- Molecular formula:C8H9NO3S
- Molecular Weight:199.23
376347-09-0
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55512-05-5
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Yield:55512-05-5 97%
Reaction Conditions:
with pyridinium chlorochromate in dichloromethane at 20; for 1 h;
Steps:
5.1.77.C
C. 3-[(MethyIsulfonyl)amino]benzaldehyde.; [3-(Hydroxymethyl) phenyl](methylsulfonyl) amine (0.42 g, 2.08 mmol) was dissolved in dichloromethane (20 mL) followed by addition of pyridinium chlorochromate (0.67 g, 3.12 mmol). The reaction was stirred at rt for IH. Filtered crude reaction through a plug of silica gel and washed with 60% EtOAc/Hex (250 mL), removed volatiles under reduced pressure to afford the title compound (0.40 g, 2.01 mmol, 97%) as a white solid. MS (ESI) m/z 200.2 [M+l]+ [00391]
References:
WO2008/51494,2008,A1 Location in patent:Page/Page column 119
![Methanesulfonamide, N-[3-(dimethoxymethyl)phenyl]-](/CAS/20210305/GIF/916059-46-6.gif)
916059-46-6
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55512-05-5
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4518-10-9
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$12.80/1g
55512-05-5
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$37.00/100mg
32087-05-1
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55512-05-5
58 suppliers
$37.00/100mg