METHYL 3-BUTENOATE synthesis
- Product Name:METHYL 3-BUTENOATE
- CAS Number:3724-55-8
- Molecular formula:C5H8O2
- Molecular Weight:100.12
35466-83-2
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3724-55-8
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$106.00/1g
Yield:3724-55-8 100%
Reaction Conditions:
with carbon monoxide;triphenylphosphine;palladium diacetate
Steps:
1 EXAMPLE 1
EXAMPLE 1 Allyl methyl carbonate (11.6 g, 0.1 mole), palladium acetate (22.4 mg, 0.1 mmole) and triphenylphosphine (78.9 mg, 0.3 mmole) were placed in a 100-mlpressure vessel equipped with magnetic stirrer. The vessel was closed and flushed with purified N2 and then charged with carbon monoxide to a pressure of 1000 psig. The vessel was heated to 100° C. while the contents were stirred. After 2 hours, the vessel was cooled to room temperature and the contents analyzed by gas chromatography. p-Diisopropylbenzene was used as standard for quantification of the product. The result showed 10.0 g of methyl 3-butenoate had been formed. The yield was accordingly 100 percent.
References:
The Dow Chemical Company US4450285, 1984, A
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3724-55-8
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40637-56-7
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35466-83-2
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201230-82-2
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3724-55-8
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3724-55-8
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