Methyl [2-(bromomethyl)phenyl]methoxycarbamate synthesis
- Product Name:Methyl [2-(bromomethyl)phenyl]methoxycarbamate
- CAS Number:151827-83-7
- Molecular formula:C10H12BrNO3
- Molecular Weight:274.11
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Yield:-
Reaction Conditions:
with N-Bromosuccinimide;2,2'-azobis(isobutyronitrile) in tetrachloromethane;Heating;
Steps:
2.4
(4) 0.1 mol of N-methoxy-N-2-methylphenylcarbamate, 0.1 mol of N-bromosuccinimide and a carbon tetrachloride solvent were added to the reactor, 0.13mol azobisisobutyronitrile, heat, after the end of the reaction by washing, drying, vacuum distillation obtained a yellow oil is methyl N-methoxy-N- (2-bromomethylphenyl) carbamate;
References:
CN106008347,2016,A Location in patent:Paragraph 0027; 0032
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