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ChemicalBook CAS DataBase List Iron phthalocyanine
132-16-1

Iron phthalocyanine synthesis

4synthesis methods
-

Yield:132-16-1 49%

Reaction Conditions:

with (NH4)2Mo2O7 in neat (no solvent)other Radiation; mixt. of O-phthalic anhydride, urea, metal salt and (NH4)2Mo2O7 irradiated in microwave oven at 460W for 8 min. the at 800W for 8 min, cooling to room temp.; washed (H2O, acetone, MeOH, 6M HCl), reflux with acetone, MeOH and CHCl3resp. about 12 h; elem. anal.;

References:

Xu, Zhanwei;Zhang, Guoxiang;Cao, Zeyuan;Zhao, Jianshe;Li, Hejun [Journal of Molecular Catalysis A: Chemical,2010,vol. 318,# 1-2,p. 101 - 105]

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