Hexachloro-1,3-butadiene synthesis
- Product Name:Hexachloro-1,3-butadiene
- CAS Number:87-68-3
- Molecular formula:C4Cl6
- Molecular Weight:260.76
127-18-4
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Yield:-
Reaction Conditions:
with zinc(II) chloride at 100; for 12 h;Autoclave;
Steps:
2 Comparative Example 2
Separately using tetrachlorethylene as raw material,81.5 g of tetrachlorethylene was weighed in a hydrothermal autoclave, 12.2 g of anhydrous zinc chloride was added at a mass fraction of 15%, reacted at a reaction temperature of 100 ° C for 12 h,The conversion of tetrachlorethylene was 24% and the selectivity of hexachloro-1,3-butadiene was 21%.
References:
CN106966859,2017,A Location in patent:Paragraph 0015; 0022
79-01-6
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87-68-3
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87-68-3
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87-68-3
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