ethyl(2-naphthyl)amine synthesis
- Product Name:ethyl(2-naphthyl)amine
- CAS Number:2437-03-8
- Molecular formula:C12H13N
- Molecular Weight:171.24
101-02-0
391 suppliers
$10.00/5g
75-04-7
404 suppliers
$10.00/20mg
135-19-3
752 suppliers
$9.00/1g
2437-03-8
25 suppliers
inquiry
Yield:2437-03-8 96%
Reaction Conditions:
in water;
Steps:
32 N-ethyl-β-naphthylamine
EXAMPLE 32 N-ethyl-β-naphthylamine 288 parts of β-naphthol, 6.6 parts of triphenyl phosphite and 115 parts of ethylamine gas are heated for 10 hours at 230° C in a pressure autoclave. The pressure is 35 atmospheres. The mixture is added to 2,000 parts of water and the batch is stirred for 30 minutes at 70° - 80° C. The lower oily phase is separated off and distilled. 328 parts of N-ethyl-β-naphthylamine of boiling point 119° - 120° C/0.1 mm Hg are obtained. This corresponds to a yield of 96% of theory.
References:
US4067903,1978,A
102-10-3
7 suppliers
inquiry
75-04-7
404 suppliers
$10.00/20mg
135-19-3
752 suppliers
$9.00/1g
2437-03-8
25 suppliers
inquiry
15205-57-9
46 suppliers
inquiry
75-04-7
404 suppliers
$10.00/20mg
135-19-3
752 suppliers
$9.00/1g
2437-03-8
25 suppliers
inquiry
64-67-5
374 suppliers
$14.00/5g
581-97-5
49 suppliers
$172.00/250mg
2437-03-8
25 suppliers
inquiry
6933-05-7
0 suppliers
inquiry