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ChemicalBook CAS DataBase List Ethyl 2-(aminomethyl)nicotinate hydrochloride
697739-11-0

Ethyl 2-(aminomethyl)nicotinate hydrochloride synthesis

3synthesis methods
75358-90-6 Synthesis
ETHYL 2-CYANOPYRIDINE-3-CARBOXYLATE

75358-90-6
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$60.00/50mg

Ethyl 2-(aminomethyl)nicotinate hydrochloride

697739-11-0
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Yield:697739-11-0 100%

Reaction Conditions:

with hydrogenchloride;hydrogen;palladium 10% on activated carbon in water; under 2585.81 Torr;

Steps:

35 Description 35: F3-ETHOXYCARBONYLPYRIDIN-2-YLLMETHANAMINIUM CHLORIDE

To a nitrogen flushed solution of Description 34 (14.27 g, 81 mmol) and conc. HC1 (15 ml) was added 10% Palladium on carbon (2 g), and the resulting mixture hydrogenated at 50 psi until HPLC and MS indicated complete conversion (approx 2 days). The catalyst was removed by filtration and the filtrate evaporated to give the title compound (17.55 g, 100%).

References:

WO2004/46133,2004,A1 Location in patent:Page 31-32