天堂网亚洲,天天操天天搞,91视频高清,菠萝蜜视频在线观看入口,美女视频性感美女视频,95丝袜美女视频国产,超高清美女视频图片

Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List EPA
10417-94-4

EPA synthesis

2synthesis methods
-

Yield:10417-94-4 98%

Reaction Conditions:

with immobilized lipase from Candida Antarctica;water in 1,4-dioxane at 55; for 3 h;Enzymatic reaction;

Steps:

2.2. Preparation of EPA acid

To a solution of the ethyl ester of EPA (200mg, 0.6mmol) in 1.7mL of dioxane, 300μL of distilled water and Novozym 435 (200mg) were added. The mixture was stirred at 55°C and 280rpm in a shaker for 3h. Then, the enzyme was separated by filtration and the solution taken to dryness under reduced pressure. The residue was purified by column chromatography (Si gel 3.9 g, from n-hexane to n-hexane/EtOAc 9:1 containing 0.1% of HCOOH, 200mL) to give pure (TLC analysis) EPA (180mg, 0.59mmol, 98% yield) as a colorless oil.

References:

Sanfilippo, Claudia;Paterna, Angela;Biondi, Daniela M.;Patti, Angela [Bioorganic Chemistry,2019,vol. 93,art. no. 103325]

EPA Related Search: