Dodecane synthesis
- Product Name:Dodecane
- CAS Number:112-40-3
- Molecular formula:C12H26
- Molecular Weight:170.33
3344-70-5
217 suppliers
$5.00/1g
112-40-3
381 suppliers
$10.00/10g
Yield:112-40-3 90%
Reaction Conditions:
with triethylamine in water at 20; for 2 h;Inert atmosphere;Irradiation;
Steps:
5 Example 5
Using CdSe QDs as a photocatalyst, 4 mL of water was added to the photocatalyst.Wherein the solubility of the catalyst is 2×10-5M,Add 1,12-dibromododecane (164 mg, 0.5 mmol)And 300 μL of triethylamine (218.1 mg, 2.16 mmol),Replace the air with an Ar atmosphere at room temperature,The LED lamp (λ > 460 nm) was irradiated for 2 h.After the reaction, diphenylacetonitrile is the internal standard.Dodecane was detected as the main product by FID-GC.The yield is as high as 90%.
References:
CN109438156,2019,A Location in patent:Paragraph 0063; 0064
143-07-7
757 suppliers
$5.00/25g
112-40-3
381 suppliers
$10.00/10g
111-82-0
417 suppliers
$6.00/25g
112-40-3
381 suppliers
$10.00/10g
106165-36-0
0 suppliers
inquiry
112-40-3
381 suppliers
$10.00/10g
13187-99-0
12 suppliers
$214.00/5g
112-40-3
381 suppliers
$10.00/10g