Cyclamic acid synthesis
- Product Name:Cyclamic acid
- CAS Number:100-88-9
- Molecular formula:C6H13NO3S
- Molecular Weight:179.24
108-91-8
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$10.00/5mL
100-88-9
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$30.00/25g
Yield:-
Reaction Conditions:
with chlorosulfonic acid in acetonitrile at 20; for 2 h;
Steps:
General procedure for synthesis of catalysts NSA 01-05, NSA 07 and NSA 08
General procedure: To a round-bottom flask containing nitrogenatedcompound (1 mmol, amine, urea or thiourea) in dry acetonitrile (3 mL), it was added chlorosulfonic acid (1 mmol) dropwise over a period of 20 min at room temperature. The reactional mixture was stirred for 2 h,and the acetonitrile was removed under vacuum to givethe catalysts.
References:
Hack, Carolina R. L.;Porciuncula, Larissa;Weber, Andressa C. H.;D’Oca, Caroline R. M.;Russowsky, Dennis;Moura, Jaqueline M.;Pinto, Luiz A. A.;D’Oca, Marcelo G. M. [Journal of the Brazilian Chemical Society,2018,vol. 29,# 11,p. 2342 - 2349]
1122-60-7
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$99.00/5g
100-88-9
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$30.00/25g
2211-64-5
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$27.00/100mg
100-88-9
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3173-53-3
241 suppliers
$24.00/25 g
100-88-9
148 suppliers
$30.00/25g