4-(4-N-PROPYLPHENYL)BENZALDEHYDE synthesis
- Product Name:4-(4-N-PROPYLPHENYL)BENZALDEHYDE
- CAS Number:93972-05-5
- Molecular formula:C16H16O
- Molecular Weight:224.3
92-52-4
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: AlCl3 / CH2Cl2 / 5 h / Ambient temperature
2: 1) hydrazine hydrate, 2) KOH / 1) diethylene glycol, 130 deg C, 1 h, 2) diethylene glycol, 130 deg C, 2 h, then 160 deg C, 3 h
3: 1) TiCl4, 2) hydroxylamine hydrochloride, pyridine / 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h
4: 71 percent / acetic anhydride / 2 h / Heating
5: Ni-Al alloy, 75percent formic acid / 8 h / Heating
References:
Ruolene, Yu. I.;Adomenas, P. V.;Sirutkaitis, R. A.;Denis, G. I. [Journal of Organic Chemistry USSR (English Translation),1984,vol. 20,p. 1187 - 1191][Zhurnal Organicheskoi Khimii,1984,vol. 20,# 6,p. 1305 - 1310]
58743-76-3
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37940-57-1
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$60.00/100mg
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10289-45-9
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![[1,1'-Biphenyl]-4-carboxaldehyde, 4'-propyl-, oxime](/CAS/20210305/GIF/93972-12-4.gif)
93972-12-4
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