3,5-DIMETHOXYBENZYL BROMIDE synthesis
- Product Name:3,5-DIMETHOXYBENZYL BROMIDE
- CAS Number:877-88-3
- Molecular formula:C9H11BrO2
- Molecular Weight:231.09
705-76-0
877-88-3
General procedure for the synthesis of 3,5-dimethoxybenzyl bromide from 3,5-dimethoxybenzyl alcohol: 3,5-dimethoxybenzyl alcohol (1 mmol) was dissolved in anhydrous benzene (15 mL) under anhydrous conditions and phosphorus tribromide (0.5 mL) was added. The reaction mixture was stirred at room temperature until the reaction was complete. The target product 3,5-dimethoxybenzyl bromide was obtained in quantitative yield by conventional post-treatment.
705-76-0
329 suppliers
$10.00/1g
877-88-3
225 suppliers
$5.00/250mg
Yield:877-88-3 100%
Reaction Conditions:
with phosphorus tribromide in benzene at 20;
Steps:
Step-II (Preparation of benzyl bromides)
General procedure: benzyl alcohols (1 mmol) in dry benzene (15 mL) and phosphorus tribromides (0.5 mL) and stirred at room temperature to get respective benzyl bromides in quantitative yields, usual work-up.
References:
Parihar, Swati;Kumar, Amit;Chaturvedi, Amit K.;Sachan, Naresh Kumar;Luqman, Suaib;Changkija, Bendangla;Manohar, Murli;Prakash, Om;Chanda;Khan, Feroz;Chanotiya;Shanker, Karuna;Dwivedi, Anila;Konwar, Rituraj;Negi, Arvind S. [Journal of Steroid Biochemistry and Molecular Biology,2013,vol. 137,p. 332 - 344]
7311-34-4
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877-88-3
225 suppliers
$5.00/250mg
1132-21-4
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$10.00/5g
877-88-3
225 suppliers
$5.00/250mg
192997-46-9
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877-88-3
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2150-37-0
302 suppliers
$6.00/5g
877-88-3
225 suppliers
$5.00/250mg