3,4-Dichloro-6-(trifluoromethyl)toluene synthesis
- Product Name:3,4-Dichloro-6-(trifluoromethyl)toluene
- CAS Number:74483-51-5
- Molecular formula:C8H5Cl2F3
- Molecular Weight:229.03
500 ml of hydrogen fluoride, 600 ml of carbon tetrachloride and 140 g of 3,4-dichlorotoluene are reacted at 110° to 115° C. and 18.5 to 19.5 bar pressure. 151 g of a stubstance containing, in addition to 79.1% by weight of 3,4-dichlorotoluene, 20.2% by weight of 2-methyl-4,5-dichloro-benzotrifluoride, are obtained, corresponding to 74% of the theoretical yield, relative to 3,4-dichlorotoluene converted.
95-75-0
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$15.00/25g
74483-51-5
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$18.00/1g
Yield:74483-51-5 74%
Reaction Conditions:
with hydrogen fluoride in tetrachloromethane;
Steps:
7 EXAMPLE 7
EXAMPLE 7 500 ml of hydrogen fluoride, 600 ml of carbon tetrachloride and 140 g of 3,4-dichlorotoluene are reacted at 110° to 115° C. and 18.5 to 19.5 bar pressure. 151 g of a stubstance containing, in addition to 79.1% by weight of 3,4-dichlorotoluene, 20.2% by weight of 2-methyl-4,5-dichloro-benzotrifluoride, are obtained, corresponding to 74% of the theoretical yield, relative to 3,4-dichlorotoluene converted.
References:
US4533777,1985,A