2'-Chloroacetophenone synthesis
- Product Name:2'-Chloroacetophenone
- CAS Number:2142-68-9
- Molecular formula:C8H7ClO
- Molecular Weight:154.59
5000-66-8
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2142-68-9
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Yield:2142-68-9 97%
Reaction Conditions:
with diethyl ether in lithium hydroxide monohydrate at 20; for 1.5 h;Schlenk technique;Irradiation;
Steps:
3. General procedure for the reaction of reductive dehalogenation
General procedure: To a 10 mL schlenk tube, 1 (0.2 mmol), H2O (1.6 mmol) and Et2O (4 mL) were added in sequence. The reaction mixture was stirred and irradiated by 40 W Kessil purple LED (390 nm) at room temperature . After the reaction was completed, the reaction mixture was purified by flash column chromatography using PE/EtOAc as the eluent to give the desired product.
References:
Zhang, Jinrong;Chen, Jiajia;Chen, Jianhui;Luo, Yanshu;Xia, Yuanzhi [Tetrahedron Letters,2022,vol. 98,art. no. 153835] Location in patent:supporting information
873-31-4
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2142-68-9
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89-96-3
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2142-68-9
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2039-87-4
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2142-68-9
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3609-45-8
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2142-68-9
408 suppliers
$6.00/10g