2-Chloro-6-methyl-4-(trifluoromethyl)pyridine synthesis
- Product Name:2-Chloro-6-methyl-4-(trifluoromethyl)pyridine
- CAS Number:22123-14-4
- Molecular formula:C7H5ClF3N
- Molecular Weight:195.57
75-16-1
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39890-98-7
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$13.00/1g
22123-14-4
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$11.00/250mg
Yield: 73%
Reaction Conditions:
iron(II) chloride in tetrahydrofuran at 20; for 2 h;Product distribution / selectivity;Inert atmosphere;
Steps:
3 Synthesis Example 3
Synthesis Example 3 In the same manner as in Synthesis Example 1, except for using 4.61 g (0.0213 mol) of 2,6-dichloro-4-trifluoromethylpyridine and using 15 mg of iron(II) chloride as a metal catalyst, 3.16 g (purity: 96.6%, yield: 73%) of 2-chloro-6-methyl-4-trifluoromethylpyridine was obtained.
References:
ISHIHARA SANGYO KAISHA, LTD. US2012/35372, 2012, A1 Location in patent:Page/Page column 4
676-58-4
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39890-98-7
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$13.00/1g
22123-14-4
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$11.00/250mg
25462-85-5
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$6.00/250mg
22123-14-4
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$11.00/250mg
22123-19-9
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$19.00/100mg
22123-14-4
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$11.00/250mg
654-49-9
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$24.73/250mgs:
22123-14-4
143 suppliers
$11.00/250mg