2-Chloro-5-aminophenol synthesis
- Product Name:2-Chloro-5-aminophenol
- CAS Number:6358-06-1
- Molecular formula:C6H6ClNO
- Molecular Weight:143.57
619-10-3
216 suppliers
$5.00/1g
6358-06-1
178 suppliers
$5.00/250mg
Yield:6358-06-1 98%
Reaction Conditions:
Pt/C in ethyl acetate
Steps:
1.b b).
b). 2-Chloro-5-aminophenol A solution of 2-chloro-5-nitrophenol (25 g, 0.14 mol) in ethyl acetate (150 mL) was treated with 5% Pt/C (250 mg) and the mixture shaken under a hydrogen atmosphere (30 psi) for 4 h. The mixture was filtered through Celiteg and the residue washed well with hot ethyl acetate. The filtrate was treated with activated charcoal and re-filtered as above. Evaporation of the ethyl acetate gave a solid (19.8 g, 98%).
References:
Dhanak, Dashyant;Knight, Steven David US2003/100580, 2003, A1
13726-14-2
166 suppliers
$12.00/1g
6358-06-1
178 suppliers
$5.00/250mg
1009-36-5
180 suppliers
$12.00/1g
6358-06-1
178 suppliers
$5.00/250mg
97-52-9
267 suppliers
$10.00/5g
6358-06-1
178 suppliers
$5.00/250mg
121-88-0
30 suppliers
$10.00/5g
6358-06-1
178 suppliers
$5.00/250mg