2-(4-Aminophenyl)ethylamine synthesis
- Product Name:2-(4-Aminophenyl)ethylamine
- CAS Number:13472-00-9
- Molecular formula:C8H12N2
- Molecular Weight:136.19
24954-67-4
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13472-00-9
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Yield:13472-00-9 100%
Reaction Conditions:
with hydrogen in methanol at 20; under 760.051 Torr;
Steps:
20.1 Step 1. 4-(2-aminoethyl)aniline
2-(4-Nitrophenypethanamine (5.0 g, 30 mmol) and Raney Ni (500 mg) were added to methanol (50 mL) and the mixture was stirred under 1 atmosphere of hydrogen overnight. The reaction mixture was filtered, Raney Ni was washed with methanol (50 mL×4), and the filtrate was dried by rotary evaporation to give 4-(2-aminoethyl)aniline (4.1 g, 30 mmol), yield: 100%.
References:
Shanghai Zhimeng Biophama Co., Ltd.;CHEN, Huanming US2019/152963, 2019, A1 Location in patent:Paragraph 0342-0344
555-21-5
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13472-00-9
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3544-25-0
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13472-00-9
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![[4-(2-AMINO-ETHYL)-PHENYL]-CARBAMIC ACID TERT-BUTYL ESTER](/CAS/GIF/457631-44-6.gif)
457631-44-6
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13472-00-9
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2922-41-0
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13472-00-9
263 suppliers
$18.00/1g