ChemicalBook CAS DataBase List [3R-(3alpha,3abeta,6alpha,7beta,8aalpha)]-hexahydro-3,6,8,8-tetramethyl-1H-3a,7-methanoazulen-5(4H)-one

[3R-(3alpha,3abeta,6alpha,7beta,8aalpha)]-hexahydro-3,6,8,8-tetramethyl-1H-3a,7-methanoazulen-5(4H)-one synthesis

2synthesis methods

Product Name:[3R-(3alpha,3abeta,6alpha,7beta,8aalpha)]-hexahydro-3,6,8,8-tetramethyl-1H-3a,7-methanoazulen-5(4H)-one
CAS Number:13794-73-5
Molecular formula:C15H24O
Molecular Weight:220.35

469-61-4 Synthesis

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[3R-(3alpha,3abeta,6alpha,7beta,8aalpha)]-hexahydro-3,6,8,8-tetramethyl-1H-3a,7-methanoazulen-5(4H)-one

13794-73-5
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: dimethylsulfide borane complex / tetrahydrofuran / 4 h
1.2: 3 h
2.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C

References:

CN112592252, 2021, A

13567-40-3
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13794-73-5
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References

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[3R-(3alpha,3abeta,6alpha,7beta,8aalpha)]-hexahydro-3,6,8,8-tetramethyl-1H-3a,7-methanoazulen-5(4H)-one synthesis