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ChemicalBook CAS DataBase List 1-Bromo-4,4,5,5,6,6,6-heptafluoro-3,3-bis(trifluoromethyl)hex-1-ene
128454-94-4

1-Bromo-4,4,5,5,6,6,6-heptafluoro-3,3-bis(trifluoromethyl)hex-1-ene synthesis

1synthesis methods
-

Yield:128454-94-4 90%

Reaction Conditions:

with tetrabutylammomium bromide in dichloromethane at 80; for 7 h;other nucleophiles possible (NaN3, NaNO2, KSCN, KCN), other solvents possible (C2H4Cl2, ethyl acetate);

References:

Rozhkov, I. N.;Igumnov, S. M.;Pletnev, S. I.;Chaplina, I. V. [Bulletin of the Academy of Sciences of the USSR Division of Chemical Science,1990,vol. 39,# 4.2,p. 856][Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya,1990,# 4,p. 951]

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