1-Ethylpiperidine synthesis
- Product Name:1-Ethylpiperidine
- CAS Number:766-09-6
- Molecular formula:C7H15N
- Molecular Weight:113.2
618-42-8
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766-09-6
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$22.00/25mL
Yield:766-09-6 20%
Reaction Conditions:
with hydrogen;PtV/titania in acetic acid at 130; under 7500.75 Torr; for 16 h;Conversion of starting material;
Steps:
Typical Run Conditions in Batch Mode; A solution of 1-acetylpiperidine in acetic acid (2 ml, 0.8 mmol) containing n-decane (0.2 mmol) was added to a reactor containing 1 mol% of reduced PtV/titania. After purging, the hydrogen pressure was brought to 10 bar and the temperature to 130°C. GC analysis of the reaction mixture after 16 h showed formation of 1-ethylpiperidine as the sole product, having a yield of 20%.
References:
AVANTIUM INTERNATIONAL B.V. WO2005/66112, 2005, A1 Location in patent:Page/Page column 8
542-28-9
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766-09-6
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111-29-5
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766-09-6
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64-19-7
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766-09-6
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766-09-6
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7179-86-4
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