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ChemicalBook--->CAS DataBase List--->69257-04-1

69257-04-1

69257-04-1 Structure

69257-04-1 Structure
IdentificationBack Directory
[Name]

N-Benzylcinchonidinium chloride
[CAS]

69257-04-1
[Synonyms]

BCDC
-hydroxy(quinolin-4-yl)
N-benzyl chlorideCinchonidine
N-BENZYLCINCHONIDINIUM CHLORIDE
N-Benzylcinchoninium chloride ,99%
N-Benzylcinchonidinium chloride ,99%
N-Benzylcinchonidinium Chloride 
N-Benzylcinchonidinium chloride, BCDC
N-BENZYLCINCHONIDINIUM CHLORIDE HYDRATE
(8S,9R)-(-)-N-BENZYLCINCHONIDINIUM CHLORIDE
(8a,9r)-1-benzyl-9-hydroxycinchonanium chloride
(8S,9R)-(-)-BENZYLCINCHONIDINIUM CHLORID E, 98%
(8S,9R)-(-)-N-Benzylcinchonidinium chloride 98%
(8S,9R)-1-Benzyl-9-hydroxycinchonan-1-ium·chloride
(8alpha,9R)-1-benzyl-9-hydroxycinchonanium chloride
N-Benzylcinchonidinium Chloride [Chiral Phase-Transfer Catalyst]
Cinchonanium, 9-hydroxy-1-(phenylmethyl)-, chloride, (8.alpha.,9R)-
(αR,1S,4α)-α-(4-Quinolyl)-1β-benzyl-5β-vinyl-1-azoniabicyclo[2.2.2]octane-2α-methanol·chloride
[EINECS(EC#)]

273-938-3
[Molecular Formula]

C26H29ClN2O
[MDL Number]

MFCD00082422
[MOL File]

69257-04-1.mol
[Molecular Weight]

420.97
Chemical PropertiesBack Directory
[Appearance]

white to light yellow crystal powde
[Melting point ]

210 °C (dec.)(lit.)
[alpha ]

-188 º (c=0.4% in H2O)
[refractive index ]

-184 ° (C=1, H2O)
[storage temp. ]

under inert gas (nitrogen or Argon) at 2-8°C
[solubility ]

soluble in Methanol
[form ]

powder to crystal
[color ]

White to Light yellow to Light orange
[optical activity]

[α]20/D 180°, c = 1.3 in H2O
[BRN ]

5421832
[InChIKey]

FCHYSBWCOKEPNQ-WOIURNJWSA-M
Hazard InformationBack Directory
[Chemical Properties]

white to light yellow crystal powde
[Purification Methods]

Dissolve the chloride in the minimum volume of H2O and add absolute Me2CO. Filter it off and dry it in a vacuum. It can also be recrystallised from hot EtOH or EtOH/Et2O. (A good chiral phase transfer catalyst-see above) [Colonna et al. J Chem Soc, Perkin Trans 1 547 1981, Imperali & Fisher J Org Chem 57 757 1992]. [Beilstein 23 H 446.] See cinchonidine below.
Safety DataBack Directory
[Hazard Codes ]

Xi
[Risk Statements ]

36/37/38
[Safety Statements ]

26-36
[RIDADR ]

UN 2811
[WGK Germany ]

3
[HS Code ]

29392000
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Potassium carbonate-->Acetone-->Calcium chloride-->Benzyl chloride-->Cinchonidine
Spectrum DetailBack Directory
[Spectrum Detail]

N-Benzylcinchonidinium chloride(69257-04-1)1HNMR
N-Benzylcinchonidinium chloride(69257-04-1)IR
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